Pharmaceutical Chemistry – Practical (ER20-12P): Lab Manual - Lab Manual of All Experiments

Practicals
1. Limit test for
● Chlorides; sulphate; Iron; heavy metals
2. Identification tests for Anions and Cations as per Indian Pharmacopoeia
3. Fundamentals of Volumetric analysis
Preparation of standard solution and standardization of Sodium
Hydroxide, Potassium Permanganate
4. Assay of the following compounds
● Ferrous sulphate- by redox titration
● Calcium gluconate-by complexometric
● Sodium chloride-by Modified Volhard's method
● Ascorbic acid by iodometry
● Ibuprofen by alkalimetry
5. Fundamentals of preparative organic chemistry
Determination of Melting point and boiling point of organic compounds
6. Preparation of organic compounds
 Benzoic acid from Benzamide
 Picric acid from Phenol
7. Identification and test for purity of pharmaceuticals
Aspirin, Caffeine, Paracetamol, Sulfanilamide
8. Systematic Qualitative analysis experiments (4 substances)